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Then again, the steady multilayer carbonaceous chars (Figure five) generated from the reaction in between HCNP and the decomposition solutions of PA66 can insulate the underlying substrate from the warmth source and slow down the two the heat and mass transfer [25]. As a result, it may be summarized that HCNP can properly Increase the flame retardancy of PA66 subsequent the gas-stage flame retardant system.
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PA66 pellets and HCNP powder were being dried for 4 h at 100 °C before extrusion. The FR-PA66 was well prepared by twin-screw extrusion response inside the choice of 260–270 °C. The check samples had been manufactured employing a TTI-95G injection molding equipment beneath 265 °C having a 180 r/min rotation speed. Figure 6 reveals the microtopography of pure PA66, HCNP, and FR-PA66. It might be witnessed from Figure 6c the HCNP microspheres ended up dispersed extra uniformly with out evident period interfaces, as well as peeling phenomenon appeared around the surface area of the microspheres (Determine 6d), indicating that the terminal carboxyl teams of PA66 were chemically bonded With all the amino teams about the surface from the microspheres over the extrusion reaction, which ruined the regularity from the surface on the microspheres (Determine 6b, clean floor and no peeling phenomenon) and led towards the core–shell separation with the microspheres (Determine 6d), confirming the event in the in situ loading reaction.